Herbal Medicine

Purpose: ユ of scull of another name for Guangdong Province well? of commission Tong chasm the monose composition of GLPS1 of pure polysaccharide constituent and GLPS3 undertakes an analysis. Method:  scull ユ well commission Tong steals?Sephacryl S-400 SF of  of  free time gel detached and rarefied GLPS1 of 2 main constituent and GLPS3, differentiate monose composition via law of the TLC after acerbity hydrolyze and HPLC law, improved 1- phenyl - 3- is methylic - ketone of Lin of 5- Bi Zun (the develop before PMP) column monose of analysis of biochemical HPLC law composes scale, use LCMS couplet to spread out with PMP of technical appraisement monose at the same time biochemical child. Result: GThe monose group of LPS1 becomes dextrose of D- of ∶ of D- manna candy half lactose of ∶ D- the monose composition of 9.228 ∶ 1.474;GLPS3 is =1 ∶ dextrose of D- of ∶ of D- manna candy ∶ D- ∶ of half lactose =1 15.9 ∶ 3.686. Conclusion: Scull ユ well commission Tong embeds 珼 of  of annals of  aperture Ju - manna candy, half lactose of D- dextrose and D- , only the scale of each monose is different.

Purpose: Criterion the courtyard embraces palm of moisture in the soil of  of She  brilliant to closely question Nai Li crouchs crab of  of evil spirit paper of С of  of You Zhuo セ to treat? to provide referenced basis to develop resource of rattan of the fruit of Chinese magnoliavine integratedly. Method: Dizzy Li crouchs monose of aurelian appearance? and few candy, the content of polysaccharide is statistical index, apply clustering statistical method undertakes comparative to its. Result: Content of 3 kinds of index is close to month of?11 of Ran of a surname daughter-in-law and the rattan that collected in July and fructification most, and single component will tell, jia Suhan measures the rattan the fruit of Chinese magnoliavine that collected in July highest, the polysaccharide content November is highest, the monose September, few candy is highest. Conclusion: Shape of Qi of flute of joint of bones lies Sou does not have   J to wring dizzy Li of brother’s son flavour to crouch You Zhuo サ  of some evil spirit foot takes an examination of? of right Yuan Zhi to be collected to decide its are optimal close period provide referenced basis.

The purpose is like the chemical composition of chinaroot greenbrier Heterosmilax Yunnanensis to undertake study to short column. The method applies a variety of color atlas technologies to undertake depart rarefied, change method and spectrum data to have structural identification through manage. The result extracts content from 95 ﹪ alcohol in Ding Chun place departs and appraisal 9 compound, it is respectively butyl - O- β - glucoside of fructose of D- Bi Nan (Ⅰ ) , to dextrose of hydroxyl benzoic acid glucoside (Ⅱ ) , lilac sour grapes candy glucoside (Ⅲ ) , 3, 2 armour of 5- oxygen radical - 4- hydroxyl - 1-O- dextrose glucoside (Ⅳ ) , 3, 2 armour of 5- oxygen radical - 4- hydroxyl - benzoic acid - O- dextrose glucoside (Ⅴ ) , carrot glucoside (Ⅵ ) , mango glucoside (Ⅶ ) , orange peel glucoside (Ⅷ ) , 5- hydroxide is methylic furfural (Ⅸ ) . These compound all fasten conclusion to get from this depart in belonging to a plant first.

The chemical composition of purpose research the rhizome of large-headed atractylodes. The method uses solvent extraction, color atlas of silica gel column or preparation are efficient fluid photograph color atlas is detached, analyse appraisal through spectrum its structure. From inside the rhizome of large-headed atractylodes as a result depart gets 12 part, it is ketone of the rhizome of Chinese atractylods respectively (Ⅰ ) , Ⅰ of the ester inside the rhizome of large-headed atractylodes (Ⅱ ) , Ⅱ of the ester inside the rhizome of large-headed atractylodes (Ⅲ ) , Ⅲ of the ester inside the rhizome of large-headed atractylodes (Ⅳ ) , the ester inside double the rhizome of large-headed atractylodes (Ⅴ ) , amine of the acyl inside the rhizome of large-headed atractylodes (Ⅵ ) , Du Song, acerbity ester of dandelion terpene mellow second (Ⅷ ) , β - acerbity ester of sweet colophony mellow second (Ⅸ ) , β - cereal steriod is mellow (Ⅹ ) , γ - Bo steriod is mellow (Ⅺ ) with uric glucoside (Ⅻ ) , use diffraction of X- single crystal corroborant the structure of the ester inside double blank art. Ⅷ , Ⅺ and Ⅻ are conclusion compound to belong to the depart in the plant to get from the rhizome of Chinese atractylods first.

The destination is right composition of chemistry of floral of Oxytropis Falcata of beans of thorn of form of sickle Tibetan medicine undertakes study. The method uses alcohol extraction, color atlas of silica gel column is detached, analyse technical appraisement through spectrum its chemistry structure. The result receives 10 compound from inside beans of thorn of form of sickle Tibetan medicine, respectively appraisal is: 7- armour oxygen base 2 hydrogen yellow ketone (Ⅰ ) , 7- hydroxyl 2 hydrogen yellow ketone (Ⅱ ) , (S)-5- hydroxyl - 7- armour oxygen base 2 hydrogen yellow ketone (Ⅲ ) , (S)-5, 2 hydroxyl of 7- 2 hydrogen yellow ketone (Ⅳ ) , 2' , shuang Qing checks 2 hydroxyl of 4'- ear ketone (Ⅴ ) , 2' , 4' , 3 hydroxyl of 4- check ear ketone (Ⅵ ) , buckthorn element (Ⅶ ) , smelly beans is alkaline (Ⅷ ) , β - cereal steriod is mellow (Ⅸ ) , β - carrot glucoside (Ⅹ ) . Conclusion above compound all is get from the depart in this plant first.

The chemical composition of bine of Celastrus Orbiculatus of cane of the snake austral purpose research. The method uses ester of second of oil aether, acetic acid, Ding Chun is opposite respectively south the alcohol extraction content of anguine rattan undertakes extractive; apply divide into equal parts of silica gel, gel to undertake iteration departing from the method to extract rarefied, the manager changes constant to determine, structure of appraisal of method of combinative UV, IR, 1H-NMR, 13C-NMR, MS. As a result depart receives 10 compound, respectively appraisal is Shan Haitang Ⅰ of A(of the ester inside 2 terpene) , (5 β , 8 α , 9 β , 10 α , 16 β ) - 16-hydroxykaurane-18-oic acid(Ⅱ ) , salicylic (Ⅲ ) , 2, 4, 3 armour of 6- oxygen radical phenol - 1-O- β - D- dextrose glucoside (Ⅳ ) , Pi Gan of different Mongolian oak (Ⅴ ) , element of Mongolian oak skin - 7-O- β - D- dextrose glucoside (Ⅵ ) , ( ) - catechu element (Ⅶ ) , . Conclusion above compound all is get from the depart in this floral rattan first, Ⅲ of compound Ⅰ ～ is this belonging to depart first in the plant get, Ⅷ of compound Ⅳ ～ gets to depart first in this plant.

The chemical composition of bud of Lonicera Macranthoides of honeysuckle of wool of purpose research grey felt. 90 ﹪ alcohol collects medicinal material of honeysuckle of wool of methodological grey felt fluid is ordinal with oil aether and extraction of ester of acetic acid second, extraction of ester of acetic acid second relapses partly column color atlas receives compound. The result departs from inside bud of honeysuckle of grey felt wool appraisal apperception of 6 black glucoside closes matter: 3- O- β - dextrose of D- Bi Nan base (1-4)- β - dextrose of D- Bi Nan base (1-3)- α - candy of buckthorn of L- Bi Nan base (1-2)- α - Arabia candy of L- Bi Nan base - glucoside of Chinese ivy black yuan - 28-O- β - dextrose of D- Bi Nan base (. Ⅲ is conclusion compound to be belonged to from honeysuckle first share in the plant, Ⅳ , Ⅴ is share from inside this plant first, Ⅵ is glucoside of the acid of neat mound fruit that shares from inside this plant first black.

The chemical composition of root of blue Indigofera Kirilowii of purpose research flowers and trees. The method uses liquid - the method such as color atlas of column of fluid extraction, silica gel, recrystallization is detached and rarefied, wait for the structure of appraisal compound according to chart of nuclear magnetic resonance, mass spectra. From flowers and trees as a result La Gen’s alcohol extracts appraisal of the depart in content the following compound: 3, 4- 2 - acyl of O-(3- nitro- third base) - dextrose α of D- Bi Nan - with β - end radical isomer makes an appointment with 3:1mixture (Ⅰ and Ⅱ ) , Ononin(7-hydroxy-4'-methoxyisoflavone-7-O- β - D-glucopyranoside, Ⅲ ) with acyl of 6-O-(3- nitro- third base) - dextrose α of D- Bi Nan - with β - end radical isomer makes an appointment with 1: The mixture of 1 (Ⅳ and Ⅴ ) . Ⅰ and Ⅱ are conclusion compound new compound, compound Ⅲ gets to belong to the depart in the plant from Mu La first, compound Ⅳ and Ⅴ are depart from La Zhong of flowers and trees first get.

Use silica gel and analyse of gel column layer, produce hill Chinese tallow tree to Guangxi (Sapium discolor(champ. ) Muell. - the chemical composition of Arg) bine branch undertakes study, from place of ester of acetic acid second depart received compound of 5 phenolic sexes, carry chemically and spectrum learn a method to part appraisal is 3, 3' , oxygen radical tan spends 3 armour of 4'- acerbity (I) , 3, oxygen radical tan spends 2 armour of 3'- acerbity - 4'-0- β - D- xylose glucoside (Ⅱ ) , sweetgrass is acerbity (Ⅲ ) , ester of acerbity second of phenol of brazilwood of brief part of a historical period (Ⅳ ) , second gallnut is acerbity (V) . Compound I-V all is get from the depart in this plant first. Had preliminary research to the active fighting bacterium of above compound, the result shows, compound Ⅲ and Ⅳ are had fight infirmly bloodsucking A.actinomycetemicomtans of unripe bacili of the companion that put a line is active, other compound does not have apparent active.