Purpose: PLC of 蜨 of ⒑ Hu digitlizes dactylogram a collection of illustrative plates, for red ginseng quality control provides a basis. Method: Law of PLC of 郒 of Mei Cong analyses red ginseng 75 ﹪ (V/V) alcohol extracts content, use post of Century SIL C18 AQ (25cm X4.6 Mm, 5 μ M) , photograph of going from place to place is 0.1 Mol/L NaH2PO4 aqueous solution - second nitrile, linear gradient wash out, detect wavelengh 203 nm, column is lukewarm (℃ of 30 ± 0.15) , measure 20 μ L into appearance. With F of index of a collection of illustrative plates of color atlas dactylogram, qualitative likeness spends SF and mensurable likeness to spend the digitlization index such as P ﹪ to undertake evaluating. Result: of Li of Zhan of charm a surname grasps miasma to carve? shares a peak 30 times certainly, announced adequately of a collection of illustrative plates of dactylogram of red ginseng HPLC exceed news feature. Conclusion: ⒌ is troubled by liver fall forward? of Yun of sell of ㄊ of ⒆ of bath of an ancient small-mouthed wine vessel of plan vertebra grandma having enough has very good precision and repeatability, comfortable Yu Gong joins quality to control.
A collection of illustrative plates of dactylogram of color atlas of concentrated juice photograph of soup of summer of purpose research smaller part. Methodological RP-HPLC method, use 4.6 Mm of × of Lichrospher C18(250 Mm, chromatographic column of 5 μ M) , binary gradient wash out, detect wavelengh is 254 Nm, it is with bird purine nucleotide consult content. The result shares 11 mutual peaks, through with contrast tasted reservation time and ultraviolet light chart are compared, 1, 2, 3, 5, 6 peaks part appraisal is is nucleotide of pyrimidine of uric pyrimidine, yellow purine, make water, second nucleotide of purine of yellow purine nucleotide, bird. The HPLC a collection of illustrative plates of medicinal material of the tuber of pinellia determined below condition of identical color atlas, its have very good dependency with soup of smaller part summer as a result. The sex of feature of dactylogram a collection of illustrative plates of soup of summer of conclusion smaller part, exclusive the gender is very strong, this method stability, reliable, reappearance is good, the quality control that can be soup of smaller part summer considers to provide reference.
Purpose: ┎ of R of core beat Ling is troubled by liver method of? of fall forward plan: P-HPLC law of 肦 of take along sth to sb, determined sample of 25 different the root of balloonflower. Color atlas condition: HYpersil C18 column (250 mm × 4.6 Mm, m) of 5 μ , photograph of going from place to place is second nitrile - 0.05 MoL/LH3PO4 system, gradient wash out, velocity of flow is 0.5 mL/min, detect wavelengh is 210 nm, column is lukewarm 30 ℃ . Result: 5 mother of Ling of ⒘ illicit whistles б adds up to Di liver? of fall forward plan finds 17 mutual peaks in all. Conclusion: Reappearance of? of horsefly of of plum any of several hot spice plants is good, can use at the appraisal of medicinal material of the root of balloonflower and evaluation, provide reliable scientific basis to control the quality of medicinal material of the root of balloonflower.
Purpose: Beard of Luo of horny v/LIT an amphora-like jar is floated by round Shi captures feature of dactylogram of the PLC that return 腍, to build definitely a collection of illustrative plates of color atlas dactylogram of pine torch medicinal material provides a basis. Method: A kind of reed of manganese of take along sth to sb identifies separate analysis of PLC of 蠬 of of Xue of border favor duck. Chromatographic column is second nitrile for photograph of flow of Hypensil ODS column; - 1 ML/min; of velocity of flow of; of aqueous solution of 0.1 ﹪ phosphoric acid detects wavelengh is 278 Nm; ginseng to be 550 nm than wavelengh. Handle information of color atlas dactylogram with clustering method, compare color atlas all dactylogram information and it is with Chinese rhubarb phenol consult the information of the 14 features peak of chromatographic peak. Result: Mei is troubled by liver fall forward plan ㄏ bumping into error is low pull the beard that jump Luo to mirror evil spirit location to cast bing4 ru4 gao1huang1 3 pure chromatographic peak get ether of armour of element of phenol of personal? pieplant, pieplant, Chinese rhubarb element affirm. Use information of dactylogram of all color atlas relatively those who use information of dactylogram of peak of color atlas feature get together kind of result is more reliable. Conclusion: Luo beard by fragrant of Xing of apricot of broken branch of Shi of actor of the beard that boil Luo of dusk of С evil spirit value carries smile Gua gourd ladle to taste? of the that have evening definitely of pine torch unripe article with definitely dactylogram feature compares the color atlas that pine torch n/med the process of preparing Chinese medicine tastes close, but have a difference.
Purpose: б of enzymatic whistle adds up to Ai to catch liver of word of of accept of ǖ of ⒑ Ni method of? of fall forward plan: 郈 of Mei Cong of take along sth to sb 18 column, second nitrile - ; of wash out of gradient of aqueous solution of 0.5 ﹪ phosphoric acid detects 1.0 mL/min of wavelengh 275 nm; velocity of flow has a test. Result: ?0 the safflower that the province produces obtained 34 color atlas to share a peak, main feature is consistent. A of element of hydroxyl safflower yellow is index composition, the content of Xinjiang safflower is highest. Conclusion: of ┭ of favour of plum ㄎ returns illicit of ┝ of Mao of collect ㄌ first a collection of illustrative plates of dactylogram of sample of safflower of? of adept male bank and index composition content determine the quality that can be used at controlling safflower medicinal material in the round.
Purpose: Predestined relationship of sell of easy ㄊ of bad news of a kind of net used for fishing or for dredging up river sludge of an old name for Japan is troubled by liver method of? of any of several hot spice plants of Chi of accurate of fall forward plan: Po of of Xi of Li of center ⒔ all glucoside of?Cs-C-Q80) looking for ┎ and adenosine, make water contrasts article contrast, use HPLC to detect method, chromatographic column: ALltima C18(250 Mm X4.6 Mm, chromatographic column of M) of 5 μ , with second nitrile - solution of 2 hydrogen Potassium is 0.04 MoL/L phosphoric acid photograph of going from place to place, gradient wash out, velocity of flow is 0.8 ml/min, determine wavelengh: 260 nm. Result: of Lu of An of of Yun of tip of of Jing of cap of take along sth to sb hey the relative standard deviation of stability of? of of Xian of Li of shoot a glance at, precision, reappearance (RSD) all is less than 3 ﹪ , below same color atlas condition, via the HPLC appearance of different type, different chromatographic column is compared, the relative standard deviation that retains time relatively is less than 5 ﹪ . Conclusion: ? of Ji of Ku of Jing ú Zhuang is exclusive the gender is strong, reappearance is good, the dactylogram a collection of illustrative plates that can serve as 100 your capsule differentiates a method.
Purpose: PLC of 親 of ⒋ billows small house digitlizes dactylogram a collection of illustrative plates. Method: Mei Cong of take along sth to sb whistle б adds up to Ai to chase after? to use 4.6mm of × of Century SIL BDS(20 Cm, column of 5 μ M) , with water of 1 ﹪ acetic acid - nitrile of second of 1 ﹪ acetic acid is photograph of going from place to place, linear gradient wash out, 1.0 ML/mL of velocity of flow, detect wavelengh 265 nm, column is lukewarm (℃ of 30 ± 0.15) , measure 10 μ L into appearance. With qualitative, ration likeness is spent and the digitlization index such as index of a collection of illustrative plates of color atlas dactylogram evaluates medicinal material quality. Result: The month cleans out of Li of another name for Taishan Mountain to grasp miasma to carve? shares dactylogram peak 31 times certainly, built HPLC of thorn slender acanthopanax to digitlize dactylogram a collection of illustrative plates. F of index of a collection of illustrative plates of dactylogram of applied color atlas and parameter of opposite index Fr prick a collection of illustrative plates of dactylogram of slender acanthopanax HPLC to different producing area exceeded news feature to undertake digitlizing evaluating. Conclusion: A collection of illustrative plates of dactylogram of PLC of 腍 of ⒌ has better precision and reappearance, apply to the quality control that pricks slender acanthopanax medicinal material.
Purpose: Male of random ┎ of partridge of happy favour of a unit of weight used in ancient China of snail of core earnestly partridge mires brown bear smoke rises abruptly ” ひ battles Qiong? method: ⒘ method of a collection of illustrative plates of dactylogram of PLC of partridge busy 腍, use even design method, with frequency of time of dosage of solvent chroma, dissolvent, extraction, extraction 4 elements, 9 levels have every factor extraction craft experiments, the requirement of optimal extraction craft that adopts technology of HPLC dactylogram a collection of illustrative plates to extract content to undertake efficiency was evaluation index to decide capillary artemisia analytic; to spend the extraction with capillary artemisia with likeness of dactylogram a collection of illustrative plates finally to what get below each craft condition. Result: 2The 5 times alcohol that measures 11.14 ﹪ , extract 90 min every time, extract 3 times. Conclusion: Liver fall forward plan exact time Ju breaks partridge green rise abruptly ” ひ small cup flinchs Fu Jia of elder brother of vomit smile kitchens?
Purpose: A collection of illustrative plates of dactylogram of PLC of 腍 of ┎ of of herd of ⒋ ┬ analyses a method, evaluate medicinal material quality. Method: AAppearance of color atlas of photograph of Gilent1100 concentrated juice, methanol of photograph of going from place to place - water (wash out of gradient of 40) of ∶ of 60 min(60 of ～ of 30 ∶ 70) , 1.0 ML/min of velocity of flow, detect wavelengh 226 nm. Result: HThe ester inside the creat in PLC dactylogram a collection of illustrative plates kind composition all has better depart, can be compared or distinguish the quality state of medicinal material of different producing area. Conclusion: Ji of of plum any of several hot spice plants scrupulously and respectfully ⒆ already the immanent quality feature that? of quadrangle of two ⒅ impossible can stress creat crude drug.
Purpose: ⒆ uglying β as kind of bag б of whistle of ┎ male mother adds up to Di liver? of fall forward plan is hemp of the founder of a school of learning differentiate reach quality control to provide a basis. Method: The ability of drug of the founder of a school of learning to different origin has 肦 P-HPLC way chromatographic column of; of research of dactylogram a collection of illustrative plates is 200 Mm of × of Dikma Diamonsil C18 4.6 Mm, 5 μ M, column is lukewarm for 35 ℃ , velocity of flow is 1.0mL/min, detect wavelengh is 326 nm, undertake gradient wash out with second nitrile and the phosphoric acid aqueous solution of 0.05 ﹪ . Result: HMain active ingredient all gets hemp of the founder of a school of learning in PLC dactylogram a collection of illustrative plates very good depart, spend an analysis to handle a result according to likeness, the medicinal material of hemp of the founder of a school of learning of 18 kinds of different origin has 17 mutual peaks, and it is better that likeness is spent. Conclusion: Take along sth to sb of of Jing any of several hot spice plants is rotten censure ⒆ uglying β as kind of bag ┎ male is troubled by liver? of fall forward plan and handy, reliable, reappearance is good.