Purpose: б of ⒏ whistle adds up to Ai to chase after? of error of ㄍ generation to plant the Chinese traditional medicine that has effect of clear hot reduce internal heat glucoside of the gardenia in preparation and the content of glucoside of the root of large-flowere skullcap. Method: Group of photograph of flow of; of chromatographic column of Ichrospher C18 of 肔 of take along sth to sb becomes A: ? phosphoric acid (53:0.2)B: Interpret?88:1; of 2) gradient wash out detects wavelengh: 240 Nm; velocity of flow: 1ML/min. Column is lukewarm: Chair? result: Zhuang Yu dips in dash forward the whistle austral dwell model small cup encloseds ground for growing trees G/mL(r=0.999 9) of paragraph of μ of 76 of ～ of?1.9 of Х straight snipe, g/mL(r=0.999 9) of μ of 10.58 ～ 423. Reclaim on average rate mix for 101.3 ﹪ 100.6 ﹪ . Conclusion: Result of? of horsefly of of plum any of several hot spice plants is accurate and reliable, reappearance is good, make clear can determine clear to heat up reduce internal heat at the same time kind Chinese traditional medicine glucoside of the gardenia in preparation and the content of glucoside of the root of large-flowere skullcap, can use at quality control.
Purpose: б of ⒏ whistle adds up to Ai to chase after? of error of ㄍ generation to plant the Chinese traditional medicine that has effect of clear hot reduce internal heat glucoside of the gardenia in preparation and the content of glucoside of the root of large-flowere skullcap. Method: Group of photograph of flow of; of chromatographic column of Ichrospher C18 of 肔 of take along sth to sb becomes A: ? phosphoric acid (53:0.2)B: Interpret?88:1; of 2) gradient wash out detects wavelengh: 240 Nm; velocity of flow: 1ML/min. Column is lukewarm: Chair? result: Zhuang Yu dips in dash forward the whistle austral dwell model small cup encloseds ground for growing trees G/mL(r=0.999 9) of paragraph of μ of 76 of ～ of?1.9 of Х straight snipe, g/mL(r=0.999 9) of μ of 10.58 ～ 423. Reclaim on average rate mix for 101.3 ﹪ 100.6 ﹪ . Conclusion: Result of? of horsefly of of plum any of several hot spice plants is accurate and reliable, reappearance is good, make clear can determine clear to heat up reduce internal heat at the same time kind Chinese traditional medicine glucoside of the gardenia in preparation and the content of glucoside of the root of large-flowere skullcap, can use at quality control.
Fat dose of heat up in a steamer calls tar the agent again (Tar) , the different position that is plant, animal more gets via high temperature carbonization Brown or black is oily account other people. It is a kind of utility extensive, the Chinese traditional medicine with special effect; its raw material is different, the method of preparation also not identical; names decide with origin of its raw material more.
Purpose: Ran? is planted in the honeysuckle extraction substance that classical craft produces green former acid, 3, 2 coffee of 5- the content difference of acid of acyl radical quinine and total green former sick at heart. Method: Magnesian Lai is? pure law, stone - sulfur law and improved stone - honeysuckle of sulfur law production extracts content, with concentrated juice photograph - law of gradient wash out determines green former acid is mixed in content of 3 kinds of extraction 3, 2 coffee of 5- the content of acid of acyl radical quinine, determine with prismatic photometry in content of 3 kinds of extraction total green former acid content. Result: 3Kind in extracting content, green former acid content is 5.03 ﹪ , 4.01 ﹪ , 5.68 ﹪ respectively, 3, acid content of quinine of 2 coffee acyl is 5- respectively 0.41 ﹪ , 0.73 ﹪ , 1.24 ﹪ , total green former acid content is 13.53 ﹪ , 19.85 ﹪ , 27.87 ﹪ respectively. Conclusion: In the honeysuckle extraction substance that law of sulfur of herd border? produces green former acid, 3, 2 coffee of 5- acid of acyl radical quinine and total green former acid content are highest.
Coronal heart revive add up to bolus the Song Dynasty of former square out is acting ” Hui Min of peace and tranquility and agent bureau square ” [1] , just should comprise by 15 gout drug, ” Chinese pharmacopoeia ” 2000 edition [2] stops the coronal heart that carry revive add up to bolus to already simplified for Su Gexiang, borneol, frankincense (make) , 5 gout crude drug comprises white sandalwood, Qing Muxiang, this medicine has wide bosom of regulating the flow of vital energy and removing obstruction to it, acetanilide effect. Fang Zhongchen contains birthwort acid in medical Qing Muxiang, because its have kidney noxiousness, already by building sweet replace (SFDA(country feeds medical inspect to note) [2004]379 date: Subtle brag care fights? of Zhui orchid drought to plant medicinal material and its preparation supervise administrative) . ” Chinese pharmacopoeia ” 2005 edition use method of gas phase color atlas sweet to this medicine borneol and building undertake content determines [3] , medical Su Gexiang undertakes differentiating or did not contain to gentleman the quantity determines, su Gexiang’s bases is cassia bark acid, although coronal heart revive add up to bolus and coronal heart revive the method that the content of acid of the cassia bark in adding up to capsule determines already had a story [4] , but the reservation time of cassia bark acid is longer (make an appointment with 20 min) , and detect only active ingredient one cassia bark is acerbity. To control coronal heart effectively revive the immanent quality that combines bolus, this experiment established RP-HPLC standard, can determine already coronal heart revive the content of acid of the cassia bark in adding up to bolus, the content of acerbity A of the birthwort in sample can determine again in the meantime, this law fast, simple, result is accurate, can evaluate coronal heart revive the quality that combines bolus, detect black wood breaks the law spicily add.
The purpose studies two kinds of chela add up to colophony A and B to be used at taking off to divide board the feasibility that La Gen extracts ion of the heavy metal in fluid. The method accuses to extract platform oneself in industrial pattern Chinese traditional medicine aspirant travel takes off heavy metal experiment, cream in order to work a collection of illustrative plates of rate, HPLC is similarly spend and heavy metal is taken off except rate to inspect index, compare the effect of two kinds of colophony to concerning index. After the result takes off heavy metal, work cream so that lead a loss under 7 ﹪ , through taking off heavy metal unit earning does the heavy metal content that cream each batches all under national set limit to. Applied colophony A takes off the likeness of HPLC a collection of illustrative plates that except heavy metal around doing creams to spend be more than 0.97, applied colophony B takes off the likeness of HPLC a collection of illustrative plates that except heavy metal around doing creams to spend very low. Conclusion colophony A suits to divide relatively board the heavy metal in fluid of blue root extraction.
The purpose chooses much to cancer of the stomach medicine to be able to bear or endure the Chinese traditional medicine that medical cell has changeover effect, for clinical fight cancer of the stomach to be able to bear or endure medicine chooses effective Chinese traditional medicine to provide a basis. The method is used 4 methylic occasionally azotic Zun salt (MTT) medicine quick experiment, detect the alcohol of grass of tongue of dandelion, reticulate millettia, tuckahoe, licorice, long-nodded pit viper, pieplant extracts content to be able to bear or endure to cell of cancer of the stomach the changeover action of property of a medicine, use art of cell drifting type to study Chinese traditional medicine is right be able to bear or endure the likely mechanism of changeover of property of a medicine. Grass of tongue of result licorice, long-nodded pit viper, pieplant extracts content can the much medicine of changeover SGC7901/VCR cell is able to bear or endure property of a medicine, its changeover multiple is respectively 1.1, 1.5, 4.6. The content of Chinese rhubarb extraction that is not cellular toxic quantity and element of mildew of Rou Gong of the medicine that change cure (DNR) couplet is used can raise SGC7901/VCR cure medicaments chroma is changed to gather inside the cell. Content of extraction of grass of tongue of conclusion licorice, long-nodded pit viper, pieplant is OK the much medicine of cell of partial changeover cancer of the stomach is able to bear or endure property of a medicine, extract content changeover effect with Chinese rhubarb the most apparent, the likelihood is Chinese traditional medicine much medicine of cell of changeover cancer of the stomach is able to bear or endure one of medical action mechanisms.
The purpose compares Pai to pull Xi Lin / Shubatan and other 4 kinds of β - inside content fights acyl amine antibacterial outside the body to clinical and detached bacterium bacterium is active. The method uses agaragar flat duple and attenuant law determines the chroma of lowermost curb bacterium of individual plant of bacterium of clinical to 151 individual plant depart. Result Pai pulls Xi Lin / Shubatan is mixed to bacterium of Ge Lanyang sex bacterium of sex of change Lan Yin all has the better active that fight bacterium. Bacterium of single born of the same parents belongs to verdigris holiday, do not move bacillus to belong to, alvine coccus belongs to pair of Pai to pull Xi Lin / Shubatan’s sensitivity is highest, sensitive rate all is 100 ﹪ , coccus of the rare bacterium, pneumonic Bai Jun that overcome thunder, grape belongs to large intestine dust to pull Xi Lin to Pai / Shubatan’s sensitivity is taller, sensitive rate is 80 ﹪ ～ 93.74 ﹪ . Coccus of the rare bacterium, pneumonic Bai Jun that overcome thunder, grape belongs to large intestine dust, bacterium of single born of the same parents belongs to verdigris holiday, do not move bacillus to belong to to two kinds of Pai preparation of enzymatic depressor compound all compares Laxilin sensitive. Conclusion Pai pulls Xi Lin / Shubatan and Pai pull Xi Lin to compare, have the stronger active that fight drug.
Purpose from 17 kinds of Chinese traditional medicine (content of monomer, extraction and inject fluid) in fast sieve singles out pair of cellular pigment P4502D6(CYP2D6) inferior model the Chinese traditional medicine that has inhibition, build tall flux to choose the technical platform that has inhibition Chinese traditional medicine to CYP2D6. The method takes microsome of bandicoot blank liver, join 17 kinds of Chinese traditional medicine respectively, HPLC law determines the Sha Fen of bougie medicaments right beauty of the CYP2D6 in bandicoot liver microsome (the metabolization rate of DM) , through the phenomenon that metabolization rate reduces preliminary sieve singles out the medicaments that can restrain the CYP2D6 in liver microsome to metabolize. The metabolization that fluid of inject of Qin of the rhizome of chuanxiong of fluid of inject of content of extraction of glucoside of element of skin of result Mongolian oak, the root of large-flowere skullcap, the bark of official magnolia, Qing Kailing, hydrochloric acid can reduce DM apparently is led (P ＜ 0.01) . Preliminary sieve singles out conclusion these 5 kinds of Chinese traditional medicine can restrain fluid of inject of Qin of the rhizome of chuanxiong of fluid of inject of content of extraction of glucoside of element of Mongolian oak skin, the root of large-flowere skullcap, the bark of official magnolia, Qing Kailing, hydrochloric acid liver microsome CYP2D6 is enzymatic active. This method can choose the technical platform that has inhibition Chinese traditional medicine to CYP2D6 active as tall flux.