Purpose: ⑴ climbs Nuo of ashamed oyster to be troubled by persimmon collate to sunlight the) such as grass of? wide money, lustre have diarrhoea, the root of herbaceous peony. Method: of Min of 〔 of cap of take along sth to sb chases after ㄐ of discharge of of paper of Ai of ⒊ of body of Ze of ⒃ of Qian of of bulbul of Jing of grave of instrument of market of ǘ source Ψ to make an appointment with ? to use law of color atlas of concentrated juice photograph to undertake to glucoside of the green former acid in sample, peony content determines. Result: Outfit of of accept of Lu of 〔 languid knocks at negative of? of Li of a side gate of an imperial palace to contrast jam-free; content determines green former acid enters kind amount to be in ～ of G of 0.206 4 μ shows good linear concern inside limits of 2.064 μ G, reclaim on average rate for 101.1 ﹪ (N=6) , RSD enters kind amount to be in for glucoside of peony of 101 ﹪ ; ～ of G of 0.373 6 μ shows good linear concern inside limits of G of 2.241 6 μ , reclaim on average rate for 99.9 ﹪ (N=6) , RSD is 0.95 ﹪ . Conclusion: ? of Shuo of of Jing any of several hot spice plants is handy, accurate it is good to reach reappearance, the quality that can regard this as preparation controls a standard.
Purpose: Collate of persimmon of V of handkerchief of charming of Zhuo of of ⒌ Qi sunlights? method: of Min of 〔 of cap of take along sth to sb chases after?TLC) to undertake to earthworm recipe grain qualitative differentiate; to use method of color atlas of concentrated juice photograph (HPLC) and law of efficient capillary electrophoresis (HPCE) is opposite respectively yellow purine of earthworm recipe grain and amber acid undertake content determines. Result: TRecipe grain is in the earthworm in LC to contrast with amino acid article, earthworm contrasts the medicinal material is relevant locally, show the spot of same color, negative contrasts jam-free. Limits is yellow purine content of earthworm recipe grain bag of 3.3 Mg/ of 1.6 mg/ bag ～ , the content limits of amber acid is bag of 35.38 mg/ of ～ of 23.58 Mg/ bag. Conclusion: ⒌ of of couch of flute of joint of bones mu ㄐ makes an appointment with タ of horsefly of of bank branny any of several hot spice plants the quality that? of courtyard of thoroughfaring green of still small ⒅ controls earthworm recipe grain effectively.
The purpose establishs the quality standard that tells sparge agent nasally. The method uses law of layer color atlas to undertake to the root of Chinese wild ginger in preparation, chrysanthemum and borneol qualitative element of the root of purple-flowered peucedanum of the Europe in differentiating; to use HPLC law to measure custom-built agent. Law of result layer color atlas can check gives the root of Chinese wild ginger, chrysanthemum and borneol; Ou Qian Hu Su in 0.0723 2 ～ G of 0.361 6 μ and peak area have good linear concern, reclaim on average rate for 98.59 ﹪ , RSD is 1.04 ﹪ . The method that conclusion establishs is handy, accurate, reliable, reappearance is good, can regard the quality of this preparation as the standard.
From FDA history of nearly 20 years looks, general every be apart 5 years or 10 years, united States Congress wants to undertake editing to concerning the relevant law of FDA, and 2007 most the FDA that lets a person fix eyes upon reforms a project, before nothing is more… than is opposite 15 years, pass ” examine and approve prescription drug to pay cost bill ” (Prescription Drug User Fee Act, PDUFA) undertakes be approvinged again (Reauthorization) .
Purpose: ⒗ benzene peddles Li ㄐ far is branny study method of the? that show any of several hot spice plants: of cap 〔 Min chases after ㄐ of discharge of of earnestly of bandit of benzene of ǘ high mountain to make an appointment with ? to use law of gas phase color atlas to undertake to menthol, borneol content determines at the same time. It is layer board with silica gel G, with oil aether (℃ of 60 ～ 90) - ester of acetic acid second (3:2) to develop an agent, with 0.5 ﹪ 2, 2 benzene of 6- Kun chloric acyl inferior amine methanol solution is color developing agent, undertook to chili element qualitative differentiate. It is the internal standard content of GC with naphthalene, in order to get together glycol (PEG)-20M is stationary phase, besmear cloth chroma is ℃ of lukewarm 150 of column of; of detector of 10 ﹪ ;HD, undertook to menthol, borneol content determines. Result: ? of of Qiong of grow of of Yi 〔 Min is tasted for trying and chili element contrasts taste the stain that presents apparently same color in same position, and negative contrasts without this stain. Below condition of GC color atlas, menthol, borneol, naphthalene gets good depart. Of menthol, borneol add appearance to reclaim rate is ordinal for 97.44 ﹪ (RSD=0.93 ﹪ ) , 98.09 ﹪ (RSD=1.26 ﹪ ) . Conclusion: Hou of Jing Shuo already? reappearance is good, can use at controlling the quality that chili rheumatism creams.
Purpose: ⒏ beats tell course of study of the cost that feed a mythical bird like the phoenix to be troubled by persimmon collate to sunlight? method: Law of LC of 肨 of take along sth to sb joins the licorice in laurel capsule to medicine made of two or more ingredients, 37, the root of red-rooted salvia and the rhizome of chuanxiong undertake qualitative differentiate, ammonium of oxalic acid of the pleasant in using HPLC law to measure custom-built agent joins content of ketone Ⅱ A with red. Result: Acerbity ammonium of licorice of? of painful ㄜ of the Kingdom of Wei of げ of ⒌ of to fold of of ⑷ of Qian of assorted of gum of Fei of Xiang of heart of word of of Yi 〔 Min is in 4 μ G and A of Ⅱ of ketone of the root of red-rooted salvia are in 0.5 ～ 0.04 ～ sex of planted agent of limits of 0.32 μ G is good, population R is 0.999 8 and 0.999 6 respectively, reclaim on average rate it is 98.9 ﹪ respectively, 97.8 ﹪ . Conclusion: ⒌ Mu treats Chong of Ji of the that show any of several hot spice plants still? is exclusive the gender is strong, can use at medicine made of two or more ingredients to join control of laurel capsule quality.
Purpose: A round flat piece of jade with a hole in its center of of ⒓ Rong is troubled by persimmon collate to sunlight? method: 肨 LC is right firm the root of remembranous milk vetch in unripe bolus, Huang Bai and giant knotweed undertake qualitative differentiate, use HPLC to undertake to glucoside of sheep of the excessive in preparation leavessing of pulse plants content determines. Color atlas condition: 肅 18 analysises column, with second nitrile - water (25:75) is photograph of going from place to place, detect wavelengh 270 nm, 1.0 mL/min of velocity of flow. Result: ? of word of 〔 Min tastes solution color atlas to be in for trying with contrast medicinal material or contrast taste the spot that shows same color locally accordingly, negative contrasts jam-free. In color atlas of concentrated juice photograph, foreign glucoside leavessing of pulse plants is in excessive sexual relationship of planted agent of limits of G of μ of 0.39 ～ 3.90 is good (R=0.999 9) , reclaim on average lead 96.1 ﹪ . Conclusion: 〔 Min chases after ò to knock at law of color atlas of photograph of concentrated juice of? of Yun of sell of ㄊ of ⒆ of of Li of a side gate of an imperial palace handy and fast, reappearance is good, this method can serve as firm the quality standard of unripe bolus.
Purpose: Collate of persimmon of Mu Aicai of ⑿ of teaching paper sunlights method of? of crowded any of several hot spice plants: of Min of 〔 of cap of take along sth to sb chases after ǘ pregnant Chinese traditional medicine of flavour of? of of of ammonia of aim of Ai of ⒊ of lofty of げ of ⒌ of lofty of dwell of ⒒ of lofty of twinkling of ┤ of favour of of Tao of elder brother of Mu Aicai undertook qualitative analysis, determine with HPLC law content of A of Ⅱ of ketone of the root of red-rooted salvia. Result: Content of 駻 of of earthen jar of げ of instrument of Mu Aicai is 0.48 ～ 0.63 mg/ piece, the extraction that impose kind reclaims rate for 99.5 ﹪ , RSD=1.08 ﹪ (﹪ of N=6); precision RSD=1.9 (﹪ of N=5); stability RSD=1.5 (N=5, inside 8 h) ; returns to equation: Y=5 729 483X-29 445, r=0.999 7, linear limits is 0.05 μ ～ 0.83 μ G. Conclusion: of Mao of ń of plum any of several hot spice plants already? reappearance is good, install can use at heart arteries and veins piece quality control.
Purpose: Core fears Lv of persimmon of deficient ū eggplant be troubled by persimmon collate to sunlight? method: Mew of ⒌ of lofty of of ⑿ of of Huo of ⒙ of of dirty of broadleaf plant of fall from the sky calls? of accurate of of Min of inclined 〔 determines to join alkaline content painstakingly with HPLC law, photograph of going from place to place is second nitrile - 0.1 mol/L phosphoric acid solution of 2 hydrogen natrium (10:90) , detect wavelengh is 210 nm. Result: Kite of accurate of 〔 Min knocks at negative of? of Li of a side gate of an imperial palace to contrast jam-free, the content with bitter alkaline ginseng determines to reclaim on average lead 98.6 ﹪ , RSD=0.80 ﹪ (N=6) . Bitter ginseng is alkaline in 6.18 μ G/mL. Sex of planted agent of limits of ～ 14.42 μ G/mL is good, correlation coefficient 0.99994. Conclusion: Method of? of Ji of Ku of Jing ú Zhuang is stable, exclusive the gender is strong, the quality that can regard this as preparation controls a method.
Room of preparation of the 411st hospital is in liberation army of vigor capsule department one kind when development develops on the foundation of traditional classics proved recipe is had enhance immune power, be able to bear or endure anoxic those who combat the effect such as exhaustion is self-restrained product, by ginseng, the root of remembranous milk vetch, defeat pink of spore of mural glossy ganoderma, black ant, the several flavour Chinese traditional medicine such as prince ginseng is comprised. This can adjust yin and yang, fill and not dry, exert oneself effect a permanent cure.